Amino acid | Storage period at 4°C | ||||
---|---|---|---|---|---|
0 days | 1 days | 3 days | 6 days | 9 days | |
P-Ser | 41.65±0.16NS | 43.53±0.30NS | 41.13±0.38NS | 41.38±0.00NS | 41.37±2.22NS |
Tau | ND | ND | ND | ND | ND |
PEA | 3.77±2.42a | 2.56±0.06ab | 4.71±3.38ab | 1.96±0.00b | 1.94±0.06b |
Urea | ND | ND | ND | ND | ND |
Asp | ND | ND | ND | ND | ND |
Thr | ND | ND | ND | ND | ND |
Ser | 13.36±0.20NS | 14.39±0.16NS | 14.78±0.08NS | 15.08±0.00NS | 8.52±8.32NS |
Glu | 231.69±0.16NS | 253.67±3.92NS | 263.51±5.28NS | 259.80±0.00NS | 260.71±7.68NS |
Sar | 163.26±3.85NS | 176.95±1.54NS | 180.53±5.84NS | 183.94±0.00NS | 181.66±12.95NS |
Gly | 31.27±1.48NS | 33.55±1.57NS | 31.60±0.82NS | 32.06±0.00NS | 33.14±0.11NS |
Ala | 83.42±3.00NS | 90.45±0.41NS | 88.02±1.24NS | 87.42±0.00NS | 93.48±2.12NS |
Cit | 128.44±14.91NS | 144.82±1.92NS | 131.87±2.79NS | 129.46±0.00NS | 153.79±3.18NS |
a-ABA | 3.73±5.28a | 7.46±0.25a | NDb | NDb | 8.44±0.68a |
Val | 12.94±0.40NS | 12.21±1.48NS | 12.31±0.52NS | 12.72±0.00NS | 11.81±0.66NS |
Cys | 325.77±2.98NS | 339.08±9.42NS | 353.67±7.68NS | 354.70±0.00NS | 354.30±8.88NS |
Met | 15.85±2.73NS | 14.40±8.23 | 16.86±0.14 | 20.82±0.00 | 15.70±0.40 |
Cysthi | 1.04±1.47NS | 1.17±1.65 | ND | 2.44±0.00 | ND |
Ile | 21.53±0.47NS | 23.34±0.34NS | 23.35±0.47NS | 23.58±0.00NS | 22.97±0.52NS |
Leu | 22.88±0.37NS | 24.61±0.35NS | 25.21±0.64NS | 24.72±0.00NS | 24.37±1.00NS |
Tyr | 27.15±0.24NS | 30.92±0.20NS | 29.91±0.01NS | 30.20±0.00NS | 29.24±1.27NS |
Phe | 64.73±0.86NS | 71.97±0.13NS | 72.27±1.82NS | 72.00±0.00NS | 72.26±2.38NS |
b-Ala | 14.84±2.52NS | 18.25±0.69NS | 16.19±3.89NS | 13.28±0.00NS | 16.32±3.51NS |
b-AiBA | 6.89±0.13NS | 7.52±0.08NS | 7.93±0.24NS | 8.10±0.00NS | 7.99±0.35NS |
g-ABA | 29.70±0.20NS | 32.27±0.10NS | 33.04±0.17NS | 33.14±0.00NS | 33.23±0.83NS |
EOHNH2 | 89.84±0.00NS | 96.08±0.48NS | 97.18±0.99NS | 96.92±0.00NS | 98.57±2.67NS |
NH3 | 123.26±0.76NS | 135.05±1.68NS | 128.54±0.31NS | 134.12±0.00NS | 138.88±3.17NS |
Hylys | ND | ND | ND | ND | ND |
Orn | 2.75±0.07NS | 2.68±0.23NS | 3.22±0.06NS | 3.10±0.00NS | 4.51±0.01NS |
Lys | 35.73±0.16NS | 39.25±0.92NS | 39.73±1.03NS | 39.82±0.00NS | 39.43±1.26NS |
1Mehis | ND | ND | ND | ND | ND |
His | 24.36±0.17NS | 26.59±0.33NS | 25.95±0.38NS | 25.86±0.00NS | 27.03±1.51NS |
3Mehis | ND | ND | ND | ND | ND |
Ans | ND | ND | ND | ND | ND |
Car | ND | ND | ND | ND | ND |
Arg | 582.24±3.25NS | 624.46±7.13NS | 639.26±4.44NS | 629.38±0.00NS | 637.33±17.83NS |
Hypro | ND | ND | ND | ND | ND |
Pro | NDNS | 11.93±8.53NS | 7.07±9.01NS | 14.18±0.00NS | 16.76±3.03NS |
TAA | 2,102.09±31.44 | 2,279.16±11.74 | 2,287.84±32.78 | 2,299.20±0.00 | 2,333.75±60.06 |
EAA | 744.53±6.58 | 797.58±1.44 | 815.21±8.41 | 809.08±0.00 | 811.47±22.98 |
EAA/TAA(%) | 0.35±0.00 | 0.35±0.00 | 0.36±0.00 | 0.35±0.00 | 0.35±0.00 |