| conditions | ||
|---|---|---|
| GC Autosampler | Headspace vial | 20 mL |
| Incubation time | 20 min | |
| Sample amount | 0.3 g | |
| Incubation temperature | 70℃ | |
| Injector temperature | 80℃ | |
| Syringe temperature | 80℃ | |
| Sample amount | 100 μL | |
| Agitation speed | 400 rpm | |
| GC Column | Capillary column | non-polar column constituted by 94% methyl, 5% phenyl, 1% vinyl silicone |
| Length of column | 15 m | |
| ID of column | 0.32 mm | |
| Column temperature | 80℃ | |
| Runtime | 30 min | |
| IMS | Ionization source | Tritium 100 MBq |
| Voltage | Positive drift | |
| Carrier gas flow(N2 gas) | 1 mL/min 2 min -> 20 mL/min 15 min -> 20 mL/min 20 min -> 1 mL/min 22 min -> 11 mL/min 30 min | |
| Drift gas flow(N2 gas) | 150 mL/min | |
| Drift tube temperature | 45℃ |