| Contents | Condition |
|---|---|
| HPLC | Shiseido Nanospace SI-2 (Shiseido, Tokyo, Japan) |
| Column | Unison UK-Amino (250×3mm, 3μm,ImtaktCo., Kyoto, Japan) |
| Mobile phase | 90% acetonitrile |
| Detector | Shodex RI-101 (Japan) |
| Column temperature | 60℃ |
| Flow rate | 0.4mL/min |
| Injection volume | 4 μL |