GCI | Agilent6890Ngaschromatograph | |
Injection | Splitless | |
Injector temp | 200℃ | |
Carrier gas | He,1.2mL/min | |
Column | Rtx-5MS(30m×0.25mm×0.25um) Rxi-17SilMS(1.5m×0.15mm×0.15um) | |
Temp. program | 40℃(2min)-4℃/min-160℃(0min) -10℃/min-280℃(5min) | |
TOFMS | Waters Micromass GCT | Premier time-of-flight(TOF) mass spectrometer |
Acquisition delay | 180 sec | |
Mass range | 35~600 u | |
Acquisition rate | 10 spectra/sec | |
Detector voltage | 1850V | |
Electron energy | 70eV | |
Ion source temperature | 200℃ |